Alternating current polarographic determination of vanadium in petroleum
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چکیده
منابع مشابه
Polarographic determination of malononitrile.
A procedure is proposed for the determination of malononitrile by differential pulse polarography in methanolic 0.1M tetraethylammonium iodide/0.001M tetramethylammonium hydroxide as the supporting electrolyte. In this medium malononitrile is chemically converted into an electroactive species. With close control of timing of the steps in the procedure the error of the method is +/-1.5% in the c...
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Polarographicdata are presented for the reduction of selenite ion in 3M sulfuric acid, 1M potassium chloride, and 1M ammonia-ammonium chloride. In these first two media two waves are obtained correspondingto the diffusion-controlled reduction of selenite ion to selenium amalgam and the adsorption of selenite ion on the mercury drop, respectively. One wave is obtained in ammonia-ammonium chlorid...
متن کاملA Direct Current Polarographic Method for the Determination of Chlorpheniramine Maleate in Pharmaceutical Preparations
A direct polarographic method for the determination of chlorpheniramine maleate in pharmaceutical preparations had been developed. The method was based on the reduction of chlorpheniramine maleate in an acidic medium (pH 1.2-4.0). The effect of pH on the polarographic wave was investigated by recording d.c. polarograms in various supporting electrolytes. The calibration graphs were rectilinear ...
متن کاملDetermination of Vanadium in Turkish
Vanadium is found in many rocks and minerals, including asphaltite. Asphaltite is one of the naturally occurring black, solid bitumens, which are soluble at heating in carbon disulfide and fuse. Asphaltite is also a solidified hydrocarbon compound derived from petroleum. Determination of vanadium in asphaltite ash was performed by microwave-acid digestion followed by inductively coupled plasma-...
متن کاملPolarographic Determination of Traces of Gold in Blood and Serum.
A polarographic method for the determination of as little as 1 pig. of gold in blood and serum samples is described. The relative error is 2.1%. After the sample is dry ashed at 550#{176}, the gold is extracted into ether as the chloride, to separate it from interfering copper and iron. A polarogram of the gold sample is obtained in 2 M potassium hydroxide. The method should be applicable to th...
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ژورنال
عنوان ژورنال: BUNSEKI KAGAKU
سال: 1965
ISSN: 0525-1931
DOI: 10.2116/bunsekikagaku.14.886